Analysis of dynamic mechanical response in torsion
File(s)
Published version
Author(s)
Type
Journal Article
Abstract
We investigate the dynamic response of industrial rubbers (styrene-butadiene random copolymers, SBR) in torsion and compare against common small amplitude oscillatory shear measurements by using a torsion rectangular fixture, a modified torsion cylindrical fixture, and a conventional parallel plate fixture, respectively, in two different rheometers (ARES 2kFRTN1 from TA Instruments, USA and MCR 702 from Anton Paar-Physica, Austria). The effects of specimen geometry (length-to-width aspect ratio) on storage modulus and level of clamping are investigated. For cylindrical specimens undergoing torsional deformation, we find that geometry and clamping barely affect the shear moduli, and the measurements essentially coincide with those using parallel plates. In contrast, a clear dependence of the storage modulus on the aspect ratio is detected for specimens having rectangular cross section. The empirical correction used routinely in this test is based on geometrical factors and can account for clamping effects, but works only for aspect ratios above a threshold value of 1.4. By employing a finite element analysis, we perform a parametric study of the effects of the aspect ratio in the cross-sectional stress distribution and the linear viscoelastic torsional response. We propose a new, improved empirical equation for obtaining accurate moduli values in torsion at different aspect ratios, whose general validity is demonstrated in both rheometers. These results should provide a guideline for measurements with different elastomers, for which comparison with dynamic oscillatory tests may not be possible due to wall slip issues.
Date Issued
2016-02-23
Date Acceptance
2016-02-01
Citation
Journal of Rheology, 2016, 60, pp.275-287
ISSN
0148-6055
Publisher
American Institute of Physics (AIP)
Start Page
275
End Page
287
Journal / Book Title
Journal of Rheology
Volume
60
Copyright Statement
© 2016 The Society of Rheology, Inc. This article may be downloaded for personal use only. Any other use requires prior permission of the author and AIP Publishing. The following article appeared in Journal of Rheology and may be found at http://dx.doi.org/10.1122/1.4941603
Subjects
Polymers
Chemical Engineering
Interdisciplinary Engineering
Mechanical Engineering
Publication Status
Published
Article Number
275