Effect of precipitation on mechanical properties in the beta-Ti alloy Ti-24Nb-4Zr-8Sn
File(s)2016_Coakley_Ti2448mech_MSEA-AAM.pdf (2.47 MB)
Accepted version
Author(s)
Coakley, JC
Rahman, KM
Vorontsov, VA
Ohnuma, M
Dye, D
Type
Journal Article
Abstract
Tensile testing and cyclic tensile loading measurements were performed on heat-treated samples of annealed Ti-2448
and cold-rolled Ti-2448. Quenching from above the β-transus produces an alloy that is highly superelastic, has ultra-low
elastic modulus (10−25 GPa) and exhibits hysteresis on loading-unloading cycles. On repeated cycling the strain energy
absorbed in each cycle decreases. Annealed Ti-2448 exhibits a stable hysteresis loop. Peaks from the α
00 phase are
observed in X-ray diffraction (XRD) patterns, thus the material is quite lean in β-stabilising additions. The alloy is
shown to be highly unstable when heat-treated. A combination of small angle X-ray scattering (SAXS), transmission
electron microscopy (TEM) and X-ray diffraction (XRD) was employed to relate the thermally induced microstructural
evolution to the change in mechanical properties. A heat-treatment of 80 ◦C to the cold-rolled material precipitated the
ω phase, causing embrittlement. Increasing the ageing temperature from 80 to 300 ◦C increased the stiffness, made the
elastic regime more linear, and further embrittled the alloy. The low temperature heat-treatments precipitate both ω
and α
00 phases. A higher temperature ageing treatment at 450 ◦C increased the yield strength to over 1GPa and caused
embrittlement, indicating co-precipitation of α and ω phases.
and cold-rolled Ti-2448. Quenching from above the β-transus produces an alloy that is highly superelastic, has ultra-low
elastic modulus (10−25 GPa) and exhibits hysteresis on loading-unloading cycles. On repeated cycling the strain energy
absorbed in each cycle decreases. Annealed Ti-2448 exhibits a stable hysteresis loop. Peaks from the α
00 phase are
observed in X-ray diffraction (XRD) patterns, thus the material is quite lean in β-stabilising additions. The alloy is
shown to be highly unstable when heat-treated. A combination of small angle X-ray scattering (SAXS), transmission
electron microscopy (TEM) and X-ray diffraction (XRD) was employed to relate the thermally induced microstructural
evolution to the change in mechanical properties. A heat-treatment of 80 ◦C to the cold-rolled material precipitated the
ω phase, causing embrittlement. Increasing the ageing temperature from 80 to 300 ◦C increased the stiffness, made the
elastic regime more linear, and further embrittled the alloy. The low temperature heat-treatments precipitate both ω
and α
00 phases. A higher temperature ageing treatment at 450 ◦C increased the yield strength to over 1GPa and caused
embrittlement, indicating co-precipitation of α and ω phases.
Date Issued
2015-12-22
Date Acceptance
2015-12-16
Citation
Materials Science and Engineering A - Structural Materials Properties Microstructure and Processing, 2015, 655, pp.399-407
ISSN
0921-5093
Publisher
Elsevier
Start Page
399
End Page
407
Journal / Book Title
Materials Science and Engineering A - Structural Materials Properties Microstructure and Processing
Volume
655
Copyright Statement
© 2015, Elsevier. Licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International http://creativecommons.org/licenses/by-nc-nd/4.0/
Sponsor
Engineering & Physical Science Research Council (EPSRC)
Rolls-Royce Plc
Defence Science and Technology Laboratory (DSTL)
Rolls-Royce Plc
Rolls-Royce Plc
Grant Number
EP/H004882/1
JSD002
DSTLX-1000068041
See Further info
5002680312
Subjects
titanium alloys
phase transformation
electron microscopy
mechanical characterisation
X-ray diffraction
aging
Publication Status
Published