Slip-hydride interactions in Zircaloy-4: Multiscale mechanical testing and characterisation
Author(s)
Wang, Siyang
Giuliani, Finn
Britton, Thomas
Type
Journal Article
Abstract
The interactions between δ-hydrides and plastic slip in a commercial zirconium alloy, Zircaloy-4, under load were studied using in situ secondary electron microscope (SEM) micropillar compression tests of single crystal samples and ex situ digital image correlation (DIC) macroscale tensile tests of polycrystalline samples. The hydrides decorate near basal planes in orientation, and for micropillars orientated for 〈a〉 basal slip localised shear at the hydride–matrix interface is favoured over slip in α-Zr matrix due to a lower shear stress required. In contrast, for pillars oriented for 〈a〉 prismatic slip the shear stress needed to trigger plastic slip within the hydride is slightly higher than the critical resolved shear stress (CRSS) for the 〈a〉 prismatic slip system. In this case, slip in the hydride is likely achieved through 〈110〉-type shear which is parallel to the activated 〈a〉-type shear in the parent matrix. At a longer lengthscale, these results are used to inform polycrystalline samples analysed using high spatial resolution DIC. Here localised interface shear remains to be a significant deformation path which can both cause and be caused by matrix slip on planes closely-oriented to the phase boundaries. Matrix slip on planes nearly perpendicular to the adjacent hydride–matrix interfaces can either result in plastic slip within the hydrides or get arrested at the interfaces, generating local stress concentration. Through these mechanisms, the presence of δ-hydrides leads to enhanced strain localisation in Zircaloy-4 early in the plastic regime.
Date Issued
2020-11-01
Date Acceptance
2020-09-08
Citation
Acta Materialia, 2020, 200, pp.537-550
ISSN
1359-6454
Publisher
Elsevier
Start Page
537
End Page
550
Journal / Book Title
Acta Materialia
Volume
200
Copyright Statement
© 2020 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved. This manuscript is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International Licence http://creativecommons.org/licenses/by-nc-nd/4.0/
Sponsor
Rolls-Royce Plc
Engineering & Physical Science Research Council (EPSRC)
Engineering & Physical Science Research Council (E
Engineering & Physical Science Research Council (E
Royal Academy Of Engineering
Grant Number
PO: 6000-00200808
EP/K034332/1
PO 2073974
146280 MAPP - EP/P006566/1
RF/129
Subjects
cond-mat.mtrl-sci
cond-mat.mtrl-sci
Materials
0204 Condensed Matter Physics
0912 Materials Engineering
0913 Mechanical Engineering
Publication Status
Published
Date Publish Online
2020-09-15