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Laboratory-based high pressure X-ray photoelectron spectroscopy: a novel & flexible reaction cell approach
File(s)
1%2E4975096.pdf (11.76 MB)
Published version
Author(s)
Kerherve, G
Regoutz, A
Bentley, D
Hood, C
Feeley, K
Type
Journal Article
Abstract
The last 10-15 years has witnessed a resurgence in the application of high pressure X-ray photoelectron spectroscopy (HPXPS), mainly through the development of new electron energy analyser designs, and the utilization of high-brilliance synchrotron radiation sources. To continue this expansion of the technique it is crucial that instruments are developed for the home-laboratory, considering that this is where the vast majority of traditional ultra-high vacuum (UHV) X-ray photoelectron spectroscopy is performed. The research presented here introduces a new addition to the field, an instrument capable of performing spectroscopy measurements from UHV through to high pressure (25 mbar), achieved using a retractable and modular reaction cell design. The ease of use, stability (of analyser, X-ray source and gas delivery etc.), as well as overall capability of the instrument will be demonstrated.
Date Issued
2017-03-01
Date Acceptance
2017-01-17
Citation
Review of Scientific Instruments, 2017, 88
URI
DOI
ISSN
1089-7623
Publisher
AIP Publishing
Journal / Book Title
Review of Scientific Instruments
Volume
88
Copyright Statement
© 2017 Author(s). All
article content, except where otherwise noted, is licensed under a Creative Commons Attribution (CC
BY) license (http://creativecommons.org/licenses/by/4.0/).
Sponsor
The Royal Society
Engineering & Physical Science Research Council (EPSRC)
Engineering & Physical Science Research Council (EPSRC)
Engineering & Physical Science Research Council (E
The Royal Society
Grant Number
UF100105
EP/K004913/1
EP/J021199/1
YEP206
UF150693
Subjects
Science & Technology
Technology
Physical Sciences
Instruments & Instrumentation
Physics, Applied
Physics
IN-SITU
ELECTRON SPECTROMETER
RANGE
XPS
PHOTOIONIZATION
INSTRUMENT
ADSORPTION
MOLECULES
CHEMISTRY
OXIDATION
Applied Physics
09 Engineering
02 Physical Sciences
03 Chemical Sciences
Publication Status
Published
Article Number
033102