Fast synchrotron X-ray tomographic quantification of dendrite evolution during the solidification of Mg-Sn alloys
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Author(s)
Type
Journal Article
Abstract
The evolution of dendritic microstructures during the solidification of a Mg-15 wt%Sn alloy was investigated in situ via fast synchrotron X-ray microtomography. To enable these in situ observations a novel encapsulation method was developed and integrated into a fast, pink beam, imaging beamline at Diamond Light Source. The dendritic growth was quantified with time using: solid volume fraction, tip velocity, interface specific surface area, and surface curvature. The influence of cooling rate upon these quantities and primary phase nucleation was investigated. The primary dendrites grew with an 18-branch, 6-fold symmetry structure, accompanied by coarsening. The coarsening process was assessed by the specific surface area and was compared with the existing models. These results provide the first quantification of dendritic growth during the solidification of Mg alloys, confirming existing analytic models and providing experimental data to inform and validate more complex numeric models.
Date Issued
2016-08-04
Date Acceptance
2016-07-23
Citation
Acta Materialia, 2016, 118, pp.260-269
ISSN
1873-2453
Publisher
Elsevier
Start Page
260
End Page
269
Journal / Book Title
Acta Materialia
Volume
118
Copyright Statement
This is an open access article under the CC BY
license (http://creativecommons.org/licenses/by/4.0/).
license (http://creativecommons.org/licenses/by/4.0/).
License URL
Subjects
Science & Technology
Technology
Materials Science, Multidisciplinary
Metallurgy & Metallurgical Engineering
Materials Science
Magnesium alloy
Dendritic growth
3-D X-ray tomography
Coarsening mechanism
Crystallographic orientation
PHASE-FIELD SIMULATIONS
WT.PERCENT CU ALLOY
IN-SITU
DIRECTIONAL SOLIDIFICATION
ALPHA-MG
MORPHOLOGICAL EVOLUTION
ORIENTATION SELECTION
SIDEBRANCH STRUCTURE
COARSENING KINETICS
GROWTH
Materials
0912 Materials Engineering
0913 Mechanical Engineering
Publication Status
Published