Electron microscope loading and in situ nanoindentation of water ice at cryogenic temperatures
Author(s)
Dubosq, Renelle
Woods, Eric
Gault, Baptiste
Best, James P
Type
Journal Article
Abstract
Interest in the technique of low temperature environmental nanoindentation has gained momentum in recent years. Low temperature indentation apparatuses can, for instance, be used for systematic measurements of the mechanical properties of ice in the laboratory, in order to accurately determine the inputs for the constitutive equations describing the rheologic behaviour of natural ice (i.e., the Glen flow law). These properties are essential to predict the movement of glaciers and ice sheets over time as a response to a changing climate. Herein, we introduce a new experimental setup and protocol for electron microscope loading and in situ nanoindentation of water ice. Preliminary testing on pure water ice yield elastic modulus and hardness measurements of 4.1 GPa and 176 MPa, respectively, which fall within the range of previously published values. Our approach demonstrates the potential of low temperature, in situ, instrumented nanoindentation of ice under controlled conditions in the SEM, opening the possibility for investigating individual structural elements and systematic studies across species and concentration of impurities to refine to constitutive equations for natural ice.
Date Issued
2023-02-10
Date Acceptance
2023-01-30
Citation
PLoS One, 2023, 18 (2), pp.1-11
ISSN
1932-6203
Publisher
Public Library of Science (PLoS)
Start Page
1
End Page
11
Journal / Book Title
PLoS One
Volume
18
Issue
2
Copyright Statement
Copyright: © 2023 Dubosq et al. This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.
License URL
Identifier
https://www.webofscience.com/api/gateway?GWVersion=2&SrcApp=PARTNER_APP&SrcAuth=LinksAMR&KeyUT=WOS:000960037400001&DestLinkType=FullRecord&DestApp=ALL_WOS&UsrCustomerID=a2bf6146997ec60c407a63945d4e92bb
Subjects
CREEP
DEFORMATION
FORCE MICROSCOPY
FRACTURE
HARDNESS
INTERFACES
Multidisciplinary Sciences
PLASTIC-FLOW
Science & Technology
Science & Technology - Other Topics
SIZE
SURFACE
TIDAL FLEXURE
Publication Status
Published
Article Number
e0281703
Date Publish Online
2023-02-10