Mechanical and microstructural investigations of tungsten and doped tungsten materials produced via powder injection molding
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Published version
Author(s)
Type
Journal Article
Abstract
The physical properties of tungsten such as the high melting point of 3420°C, the high strength and thermal conductivity, the low thermal expansion and low erosion rate make this material attractive as a plasma facing material. However, the manufacturing of such tungsten parts by mechanical machining such as milling and turning is extremely costly and time intensive because this material is very hard and brittle.
Powder Injection Molding (PIM) as special process allows the mass production of components, the joining of different materials without brazing and the creation of composite and prototype materials, and is an ideal tool for scientific investigations.
This contribution describes the characterization and analyses of prototype materials produced via PIM. The investigation of the pure tungsten and oxide or carbide doped tungsten materials comprises the microstructure examination, element allocation, texture analyses, and mechanical testing via four-point bend (4-PB). Furthermore, the different materials were characterized by high heat flux (HHF) tests applying transient thermal loads at different base temperatures to address thermal shock and thermal fatigue performance. Additionally, HHF investigations provide information about the thermo-mechanical behavior to extreme steady state thermal loading and measurements of the thermal conductivity as well as oxidation tests were done.
Post mortem analyses are performed quantifying and qualifying the occurring damage with respect to reference tungsten grades by metallographic and microscopical means.
Powder Injection Molding (PIM) as special process allows the mass production of components, the joining of different materials without brazing and the creation of composite and prototype materials, and is an ideal tool for scientific investigations.
This contribution describes the characterization and analyses of prototype materials produced via PIM. The investigation of the pure tungsten and oxide or carbide doped tungsten materials comprises the microstructure examination, element allocation, texture analyses, and mechanical testing via four-point bend (4-PB). Furthermore, the different materials were characterized by high heat flux (HHF) tests applying transient thermal loads at different base temperatures to address thermal shock and thermal fatigue performance. Additionally, HHF investigations provide information about the thermo-mechanical behavior to extreme steady state thermal loading and measurements of the thermal conductivity as well as oxidation tests were done.
Post mortem analyses are performed quantifying and qualifying the occurring damage with respect to reference tungsten grades by metallographic and microscopical means.
Date Issued
2015-08-14
Date Acceptance
2015-04-30
Citation
Nuclear Materials and Energy, 2015, 3-4, pp.22-31
ISSN
2352-1791
Publisher
Elsevier
Start Page
22
End Page
31
Journal / Book Title
Nuclear Materials and Energy
Volume
3-4
Copyright Statement
© 2015 The Authors. This is an open access article under the CC BY-NC-ND license
(http://creativecommons.org/licenses/by-nc-nd/4.0/).
(http://creativecommons.org/licenses/by-nc-nd/4.0/).
Publication Status
Published