In-situ digital image correlation for fracture analysis of oxides formed on zirconium alloys
File(s)In_situ_Oxide_Strength_CorrosionScience.pdf (1.23 MB)
Accepted version
Author(s)
Platt, P
Lunt, D
Polatidis, E
Wenman, MR
Preuss, M
Type
Journal Article
Abstract
Repeated breakdown of the protective oxide layer can be a key factor in the oxidation of zirconium alloys. Hence, accurate measurement of the oxide fracture strength is crucial for simulating the oxidation of these alloys. High resolution digital image correlation was applied to SEM images taken during in-situ tensile loading of oxidised ZIRLOTM. Bi-axial strain measurements obtained during crack formation in the oxide films were converted into stress, and fitted to Weibull distributions to predict the oxide failure strength. Analysis highlights the impact of surface roughness. Samples polished prior to oxidation gave a fracture strength of ∼1.6 GPa.
Date Issued
2016-05-17
Date Acceptance
2016-05-16
Citation
Corrosion Science, 2016, 111, pp.344-351
ISSN
0010-938X
Publisher
Elsevier
Start Page
344
End Page
351
Journal / Book Title
Corrosion Science
Volume
111
Copyright Statement
© 2016 Elsevier. Licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International http://creativecommons.org/licenses/by-nc-nd/4.0/
Subjects
Science & Technology
Technology
Materials Science, Multidisciplinary
Metallurgy & Metallurgical Engineering
Materials Science
Zirconium
SEM
XRD
Oxidation
Effects of strain
DIC
TRANSMISSION ELECTRON-MICROSCOPY
HIGH-TEMPERATURE OXIDATION
MECHANICAL-PROPERTIES
INTERFACE ROUGHNESS
CORROSION KINETICS
CLADDING ALLOYS
ZR ALLOYS
DEGRADATION
DIFFRACTION
ZIRCALOY-4
Energy
0912 Materials Engineering
0905 Civil Engineering
0913 Mechanical Engineering
Publication Status
Published